An interference on the lead L-alpha line of GXR3 is due to the K alpha line from 4,000 ppm arsenic. The high copper concentration (6,500 ppm) in GXR4 interferes with both the zinc K alpha line and background measured at 40.5° 2θ. Attempts to correct element counts with background taken at 40.5° and 46.5° 2θ or using the tungsten X-ray tube target radiation as an internal standard were not
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